Standard Swedish standard · SS-EN 17683:2023

Animal feeding stuffs - Methods of sampling and analysis - Determination of pyrrolizidine alkaloids in animal feeding stuff by LC-MS/MS

Status: Valid

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Standard Swedish standard · SS-EN 17683:2023

Animal feeding stuffs - Methods of sampling and analysis - Determination of pyrrolizidine alkaloids in animal feeding stuff by LC-MS/MS
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Scope
This document specifies a method for the quantitative determination of pyrrolizidine alkaloids (PA) in the concentration ranges shown in Table 1 in complete and supplementary feed and in forages by liquid chromatography tandem mass spectrometry (LC-MS/MS) after solid phase extraction (SPE) clean-up.

Table 1 - Summary of concentration ranges per PA tested in the collaborative trial

NOTE 1 A second method was part of the method validation collaborative main trial. For this method PA-N-Oxides are reduced by adding zinc powder to the extract of the feed material. The following steps correspond to the first and main method. Quantitative results for each PA except the otonecine type PA senkirkine represent the sum of the free PA base and its corresponding N-oxide.
NOTE 2 Due to insufficient numbers of data for some analyte-matrix combinations statistical evaluation was not valid for standardization. Received data indicated the methods applicability in experienced laboratories with appropriate quality assurance measures. Therefore, the method description is included as an informative annex (Annex D).

Subjects

Animal feeding stuffs (65.120)


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Standard Swedish standard · SS-EN 17683:2023

Animal feeding stuffs - Methods of sampling and analysis - Determination of pyrrolizidine alkaloids in animal feeding stuff by LC-MS/MS
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Price: 1 465 SEK
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PDF

Price: 1 465 SEK
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Product information

Language: English

Written by: Svenska institutet för standarder

International title:

Article no: STD-80041558

Edition: 1

Approved: 3/6/2023

No of pages: 72